/img alt="Imagem da capa" class="recordcover" src="""/>
Tese
Aço inoxidável nanoestruturado produzido via soldagem a arco elétrico.
Manufacturing methods of nanostructured stainless-steel composites (NSSC) have not yet been developed with industrial applicability. To overcome this shortage, the possibility of incorporating nanoparticles by electric arc welding was investigated, using a tubular rod filled with nanostructured flux...
Autor principal: | LOAYZA, Cristhian Ricardo |
---|---|
Grau: | Tese |
Idioma: | por |
Publicado em: |
Universidade Federal do Pará
2022
|
Assuntos: | |
Acesso em linha: |
http://repositorio.ufpa.br:8080/jspui/handle/2011/13872 |
Resumo: |
---|
Manufacturing methods of nanostructured stainless-steel composites (NSSC) have not yet been developed with industrial applicability. To overcome this shortage, the possibility of incorporating nanoparticles by electric arc welding was investigated, using a tubular rod filled with nanostructured flux composed of multi-walled carbon nanotubes
(MWCNT) and 304L stainless steel particles. This flux was manufactured by two different methods: mechanical alloying (MA) and chemical treatment (CT) with hydrogen peroxide. The second showed more promising results using control of kinetic parameters of time and
temperature, obtaining a lower degree of amorphous carbon, impurities, and crystalline defects, increasing their crystallinity and interaction of the nanotubes with the metallic matrix. MWCNT incorporation decreased the grain size by 64% when compared to the stainless-steel coating, possessing an austenitic matrix with carbide precipitation in the interdendritic spaces and grain boundaries. The microhardness increased 45% and the rate of erosion by vibratory cavitation decreased 64%, in relation to the AISI 304L coating. Additionally, XRD analyses showed a reduction of the γ{200} phase and a growth of γ{111} after the cavitation process. The method of manufacture of the nanocomposites proved to be
economically viable and with the possibility of immediate application on a large scale. |